Journal of Nanotechnology & Advanced Materials
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Journal

Journal of Nanotechnology & Advanced Materials


Volume
& Issue

Volume 5, Issue 1


Published
on

January 1, 2017


Pages

33-39


DOI

Article

Effect of Calcination Temperature on Magnetic and Electrical Properties of BiFeO$_3$ Nanoparticles Prepared By Sol-Gel Method

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Authors

E. M. M. Ibrahim Affiliation:
Physics Department, Faculty of Science, Sohag University, Sohag 82524, Egypt
, G. Farghal* Affiliation:
Physics Department, Faculty of Science, Sohag University, Sohag -82524, Egypt
, Mai M. Khalaf Affiliation:
Chemistry Department, Faculty of Science, Sohag University, 82524 Sohag, Egypt
and Hany M. Abd El-Lateef Affiliation:
Chemistry Department, Faculty of Science, Sohag University, Sohag -82524, Egypt


Abstract

In this work, a BiFeO$_3$ nanoparticle was synthesized by sol–gel method followed by calcination at different temperature 300, 400 and 500 $^\\\\circ$C. Effect of calcination temperature on the structure, morphology, electrical and magnetic properties was studied by using x–ray diffraction, scanning electron microscopy, electrical conductivity measurements and vibrating sample magnetometer, respectively. Structural analysis revealed a typical rhombohedral phase of the prepared BiFeO$_3$ nanoparticles. Scanning electron microscope investigations show that the materials are mesoporous nature with average particle size ~ (52) nm. The magnetic measurement shows significant enhancement of the ferromagnetism with the increasing of the calcination temperature which may be mainly attributed to the crystallinity improvement and the change of the oxygen vacancies content. The DC electrical resistivity measurement was carried out by the two–probe method. The temperature dependence of resistivity behavior shows typical semiconductor features for the synthesized nanoparticles.


Keywords

BiFeO3 nanoparticles, magnetic properties, electrical properties, sol-gel, antiferromagnetic


Citation

Ibrahim, E. M. M., Farghal, G., Khalaf, M. M., & Abd El-Lateef, H. M. (2017). Effect of calcination temperature on magnetic and electrical properties of BiFeO$_3$ nanoparticles prepared by sol-gel method. Journal of Nanotechnology & Advanced Materials, 5(1), 33–39. https://doi.org/10.18576/jnam/050105

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